Assessing the Potential of Biochars Prepared by Steam-Assisted Slow Pyrolysis for CO2 Adsorption and Separation.
Identifieur interne : 001047 ( Main/Exploration ); précédent : 001046; suivant : 001048Assessing the Potential of Biochars Prepared by Steam-Assisted Slow Pyrolysis for CO2 Adsorption and Separation.
Auteurs : Valentina Gargiulo [Italie] ; Alicia Gomis-Berenguer [France] ; Paola Giudicianni [Italie] ; Conchi O. Ania [France] ; Raffaele Ragucci [Italie] ; Michela Alfè [Italie]Source :
- Energy & fuels : an American Chemical Society journal [ 0887-0624 ] ; 2018.
Abstract
The potentialities in the use of biochars prepared by steam-assisted slow pyrolysis as adsorbents of gases of strategic interest (N2, CO2, and CH4) and their mixtures were explored. The biochars prepared from Populus nigra wood and cellulose fibers exhibited a narrow microporosity, with average pore sizes ranging between 0.55 and 0.6 nm. The micropore volume increased with the pyrolysis temperature, allowing CO2 and CH4 uptakes at room temperature between 1.5 and 2.5 mmol/g and between 0.1 and 0.5 mmol/g, respectively. These values are in line with those from the literature on biomass-derived carbon-based materials, exhibiting much higher porous features than those reported herein. As for the separation of CO2/N2 and CO2/CH4 gas mixtures, data showed that the prepared biochars exhibited good selectivities for CO2 over both N2 and CH4: between ca. 34 and 119 for a CO2/N2 mixture in typical post-combustion conditions (15:85, v/v) and between 14 and 34 for a CO2/CH4 mixture typical of natural gas upgrading (30:70, v/v).
DOI: 10.1021/acs.energyfuels.8b01058
PubMed: 30364494
PubMed Central: PMC6196957
Affiliations:
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Ania</name><affiliation wicri:level="4"><nlm:affiliation>POR2E Group, CEMHTI CNRS (UPR 3079), Université d'Orléans, 45071 Orléans, France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>POR2E Group, CEMHTI CNRS (UPR 3079), Université d'Orléans, 45071 Orléans</wicri:regionArea><placeName><region type="region" nuts="2">Centre-Val de Loire</region><region type="old region" nuts="2">Région Centre</region><settlement type="city">Orléans</settlement></placeName><orgName type="university">Université d'Orléans</orgName></affiliation></author><author><name sortKey="Ragucci, Raffaele" sort="Ragucci, Raffaele" uniqKey="Ragucci R" first="Raffaele" last="Ragucci">Raffaele Ragucci</name><affiliation wicri:level="1"><nlm:affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</nlm:affiliation><country xml:lang="fr">Italie</country><wicri:regionArea>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli</wicri:regionArea><wicri:noRegion>80126 Napoli</wicri:noRegion></affiliation></author><author><name sortKey="Alfe, Michela" sort="Alfe, Michela" uniqKey="Alfe M" first="Michela" last="Alfè">Michela Alfè</name><affiliation wicri:level="1"><nlm:affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</nlm:affiliation><country xml:lang="fr">Italie</country><wicri:regionArea>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli</wicri:regionArea><wicri:noRegion>80126 Napoli</wicri:noRegion></affiliation></author></analytic><series><title level="j">Energy & fuels : an American Chemical Society journal</title><idno type="ISSN">0887-0624</idno><imprint><date when="2018" type="published">2018</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The potentialities in the use of biochars prepared by steam-assisted slow pyrolysis as adsorbents of gases of strategic interest (N<sub>2</sub>, CO<sub>2</sub>, and CH<sub>4</sub>) and their mixtures were explored. The biochars prepared from <i>Populus nigra</i> wood and cellulose fibers exhibited a narrow microporosity, with average pore sizes ranging between 0.55 and 0.6 nm. The micropore volume increased with the pyrolysis temperature, allowing CO<sub>2</sub> and CH<sub>4</sub> uptakes at room temperature between 1.5 and 2.5 mmol/g and between 0.1 and 0.5 mmol/g, respectively. These values are in line with those from the literature on biomass-derived carbon-based materials, exhibiting much higher porous features than those reported herein. As for the separation of CO<sub>2</sub>/N<sub>2</sub> and CO<sub>2</sub>/CH<sub>4</sub> gas mixtures, data showed that the prepared biochars exhibited good selectivities for CO<sub>2</sub> over both N<sub>2</sub> and CH<sub>4</sub>: between ca. 34 and 119 for a CO<sub>2</sub>/N<sub>2</sub> mixture in typical post-combustion conditions (15:85, v/v) and between 14 and 34 for a CO<sub>2</sub>/CH<sub>4</sub> mixture typical of natural gas upgrading (30:70, v/v).</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">30364494</PMID><DateRevised><Year>2019</Year><Month>12</Month><Day>28</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Print">0887-0624</ISSN><JournalIssue CitedMedium="Print"><Volume>32</Volume><Issue>10</Issue><PubDate><Year>2018</Year><Month>Oct</Month><Day>18</Day></PubDate></JournalIssue><Title>Energy & fuels : an American Chemical Society journal</Title><ISOAbbreviation>Energy Fuels</ISOAbbreviation></Journal><ArticleTitle>Assessing the Potential of Biochars Prepared by Steam-Assisted Slow Pyrolysis for CO<sub>2</sub> Adsorption and Separation.</ArticleTitle><Pagination><MedlinePgn>10218-10227</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1021/acs.energyfuels.8b01058</ELocationID><Abstract><AbstractText>The potentialities in the use of biochars prepared by steam-assisted slow pyrolysis as adsorbents of gases of strategic interest (N<sub>2</sub>, CO<sub>2</sub>, and CH<sub>4</sub>) and their mixtures were explored. The biochars prepared from <i>Populus nigra</i> wood and cellulose fibers exhibited a narrow microporosity, with average pore sizes ranging between 0.55 and 0.6 nm. The micropore volume increased with the pyrolysis temperature, allowing CO<sub>2</sub> and CH<sub>4</sub> uptakes at room temperature between 1.5 and 2.5 mmol/g and between 0.1 and 0.5 mmol/g, respectively. These values are in line with those from the literature on biomass-derived carbon-based materials, exhibiting much higher porous features than those reported herein. As for the separation of CO<sub>2</sub>/N<sub>2</sub> and CO<sub>2</sub>/CH<sub>4</sub> gas mixtures, data showed that the prepared biochars exhibited good selectivities for CO<sub>2</sub> over both N<sub>2</sub> and CH<sub>4</sub>: between ca. 34 and 119 for a CO<sub>2</sub>/N<sub>2</sub> mixture in typical post-combustion conditions (15:85, v/v) and between 14 and 34 for a CO<sub>2</sub>/CH<sub>4</sub> mixture typical of natural gas upgrading (30:70, v/v).</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Gargiulo</LastName><ForeName>Valentina</ForeName><Initials>V</Initials><AffiliationInfo><Affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Gomis-Berenguer</LastName><ForeName>Alicia</ForeName><Initials>A</Initials><AffiliationInfo><Affiliation>POR2E Group, CEMHTI CNRS (UPR 3079), Université d'Orléans, 45071 Orléans, France.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Giudicianni</LastName><ForeName>Paola</ForeName><Initials>P</Initials><AffiliationInfo><Affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Ania</LastName><ForeName>Conchi O</ForeName><Initials>CO</Initials><AffiliationInfo><Affiliation>POR2E Group, CEMHTI CNRS (UPR 3079), Université d'Orléans, 45071 Orléans, France.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Ragucci</LastName><ForeName>Raffaele</ForeName><Initials>R</Initials><AffiliationInfo><Affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Alfè</LastName><ForeName>Michela</ForeName><Initials>M</Initials><AffiliationInfo><Affiliation>Istituto di Ricerche sulla Combustione (IRC), Consiglio Nazionale delle Ricerche (CNR), Piazzale Vincenzo Tecchio 80, 80126 Napoli, Italy.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2018</Year><Month>06</Month><Day>08</Day></ArticleDate></Article><MedlineJournalInfo><Country>United States</Country><MedlineTA>Energy Fuels</MedlineTA><NlmUniqueID>100971627</NlmUniqueID><ISSNLinking>0887-0624</ISSNLinking></MedlineJournalInfo><CoiStatement>The authors declare no competing financial interest.</CoiStatement></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2018</Year><Month>03</Month><Day>27</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2018</Year><Month>06</Month><Day>01</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2018</Year><Month>10</Month><Day>27</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2018</Year><Month>10</Month><Day>27</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2018</Year><Month>10</Month><Day>27</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">30364494</ArticleId><ArticleId IdType="doi">10.1021/acs.energyfuels.8b01058</ArticleId><ArticleId IdType="pmc">PMC6196957</ArticleId></ArticleIdList><pmc-dir>pmcsd</pmc-dir>
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